Reference Substances and Infrared Reference Spectra for Pharmacopoeial Analysis (WHO Technical Report Series, No. 885, 1999: Annex 3)
(1999; 117 pages)
Table des matières
Afficher le documentPreface1
Ouvrir ce répertoire et afficher son contenu1. Compilation of national, regional and international reference substances and infrared reference spectra
Fermer ce répertoire2. General guidelines for the establishment, maintenance and distribution of chemical reference substances - Reprint from WHO Technical Report Series, No. 885, 1999: Annex 3
Afficher le documentIntroduction
Fermer ce répertoirePart A. Primary chemical reference substances
Afficher le document1. Assessment of need for the establishment of chemical reference substances
Afficher le document2. Obtaining source material
Ouvrir ce répertoire et afficher son contenu3. Evaluation of chemical reference substances
Fermer ce répertoire4. Chemical and physical methods used in evaluating chemical reference substances
Afficher le document4.1 Methods used to verify the identity of chemical reference substances
Fermer ce répertoire4.2 Methods used to determine the purity of chemical reference substances
Afficher le document4.2.1 Separation techniques
Afficher le document4.2.2 Methods based on intrinsic thermodynamic properties
Afficher le document4.2.3 Other methods
Afficher le document5. Assignment of content
Ouvrir ce répertoire et afficher son contenu6. Handling and distribution of chemical reference substances
Afficher le documentPart B. Secondary chemical reference substances
Afficher le documentReferences
Afficher le documentBack cover
 
4.2 Methods used to determine the purity of chemical reference substances

The analytical methods to be employed in examining a substance should be considered in relation to its intended use. These analytical methods may be divided into three broad categories: those that require comparison with an external chemical reference substance (e.g. chromatographic or spectrophotometric methods), those that depend solely on an intrinsic dynamic property (e.g. phase solubility analysis and differential scanning calorimetry) and other methods.

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Dernière mise à jour: le 24 avril 2012